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Synthesis of nitrogen-doped ordered mesoporous carbons for catalytic dehydrochlorination of 1,2-dichloroethane
Xu, Jinming; Zhao, Xiaochen; Wang, Aiqin; Zhang, Tao
Source PublicationCARBON
2014-12-01
DOI10.1016/j.carbon.2014.09.004
Volume80Pages:610-616
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Physical ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Materials Science
WOS KeywordVINYL-CHLORIDE ; CO2 CAPTURE ; FABRICATION ; POLYMERS ; POLYACRYLONITRILE ; PERFORMANCE ; TEMPLATES ; PYROLYSIS ; FIBER
AbstractNitrogen-doped ordered mesoporous carbons (N-OMCs) were prepared via a two-step approach, using resorcinol (R) and formaldehyde (F) as the carbon precursor and dicyandiamide (DCD) as the nitrogen precursor. In this approach, dicyandiamide, formaldehyde and resorcinol were pre-polymerized in the first step using a basic catalyst to produce DCD-RF resol. The DCD-RF resol was mixed with a solution of triblock copolymer Pluronic P127 followed by the addition of an acid catalyst to facilitate the self-assembly and condensation in the second step. After calcination, N-OMCs were obtained and further characterized by nitrogen sorption, X-ray diffraction (XRD), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). The well-prepared N-OMCs were evaluated for the catalytic dehydrochlorination of 1,2-dichloroethane and exhibited superior catalytic performances and excellent stability over 72 h. (C) 2014 Elsevier Ltd. All rights reserved.
Language英语
WOS IDWOS:000344132400067
Citation statistics
Cited Times:20[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/145910
Collection中国科学院大连化学物理研究所
AffiliationChinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Xu, Jinming,Zhao, Xiaochen,Wang, Aiqin,et al. Synthesis of nitrogen-doped ordered mesoporous carbons for catalytic dehydrochlorination of 1,2-dichloroethane[J]. CARBON,2014,80:610-616.
APA Xu, Jinming,Zhao, Xiaochen,Wang, Aiqin,&Zhang, Tao.(2014).Synthesis of nitrogen-doped ordered mesoporous carbons for catalytic dehydrochlorination of 1,2-dichloroethane.CARBON,80,610-616.
MLA Xu, Jinming,et al."Synthesis of nitrogen-doped ordered mesoporous carbons for catalytic dehydrochlorination of 1,2-dichloroethane".CARBON 80(2014):610-616.
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