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One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography
Song, Zhihua1,2; Duan, Chunfeng1; Shi, Meng1,2; Li, Shenghong1; Guan, Yafeng1
KeywordZro2 Coated Sio2 Surfactant-free D-fructose 1 6-bisphosphate Hydrophilic Interaction Chromatography
Source PublicationJOURNAL OF CHROMATOGRAPHY A
2017-11-03
DOI10.1016/j.chroma.2017.09.046
Volume1522Pages:30-37
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Life Sciences & Biomedicine ; Physical Sciences
WOS SubjectBiochemical Research Methods ; Chemistry, Analytical
WOS Research AreaBiochemistry & Molecular Biology ; Chemistry
WOS KeywordHPLC SEPARATION ; BONDED SILICA ; PERFORMANCE ; SPHERES ; NANOPARTICLES ; RETENTION
AbstractIn this study, ZrO2 layer coated silica microspheres (ZrO2/SiO2) were successfully prepared by a facile one-step surfactant-free hydrothermal route under low pH condition. The synthesized ZrO2/SiO2 material was then modified with D-fructose 1, 6-bisphosphate (FDP) to improve the chromatographic separation property of the material. Fused-silica capillary columns were prepared with the modified material for evaluation. Phenolic, nucleobases and alkaloids compounds in hydrophilic interaction chromatographic (HILIC) mode showed symmetrical peaks. The FDP-ZrO2/SiO2 stationary phase showed better performance than ZrO2/SiO2 packing material and demonstrated great potential for application in HILIC mode. (C) 2017 Elsevier B.V. All rights reserved.
Language英语
WOS IDWOS:000413383200005
Citation statistics
Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/149767
Collection中国科学院大连化学物理研究所
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, CAS Key Lab Separat Sci Analyt Chem, 457 Zhongshan Rd, Dalian 116023, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100039, Peoples R China
Recommended Citation
GB/T 7714
Song, Zhihua,Duan, Chunfeng,Shi, Meng,et al. One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2017,1522:30-37.
APA Song, Zhihua,Duan, Chunfeng,Shi, Meng,Li, Shenghong,&Guan, Yafeng.(2017).One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography.JOURNAL OF CHROMATOGRAPHY A,1522,30-37.
MLA Song, Zhihua,et al."One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography".JOURNAL OF CHROMATOGRAPHY A 1522(2017):30-37.
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