DICP OpenIR
One-pot synthesis of 2-hydroxymethyl-5-methylpyrazine from renewable 1,3-dihydroxyacetone
Song, Lei1,2; Zheng, Mingyuan2; Pang, Jifeng2; Sebastian, Joby2; Wang, Wentao2; Qu, Minjie1; Zhao, Jian1; Wang, Xinhong1; Zhang, Tao2
刊名GREEN CHEMISTRY
2017-08-07
DOI10.1039/c7gc00578d
19期:15页:3515-3519
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
关键词[WOS]REDUCTIVE AMINATION ; PRIMARY AMINES ; ETHYLENE-GLYCOL ; CATALYSTS ; ACID ; 2-METHYLPYRAZINE ; CONVERSION ; OXIDATION ; PYRAZINE ; AMMONIA
英文摘要An efficient and green method for the synthesis of 2-hydroxymethyl-5-methylpyrazine was achieved from biomass derived 1,3-dihydroxyacetone and diammonium phosphate via a one-pot reaction. The product yield was as high as 72% under optimized conditions of pH = 8.0-9.1 at 90 degrees C for 1 hour in a dioxane and water mixture as a solvent. A possible reaction mechanism was proposed according to the reaction kinetics, NMR and in situ ATR-IR characterization studies.
语种英语
WOS记录号WOS:000406615800005
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/149951
专题中国科学院大连化学物理研究所
作者单位1.Dalian Polytech Univ, Mat Sci & Engn, Dalian 116034, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
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GB/T 7714
Song, Lei,Zheng, Mingyuan,Pang, Jifeng,et al. One-pot synthesis of 2-hydroxymethyl-5-methylpyrazine from renewable 1,3-dihydroxyacetone[J]. GREEN CHEMISTRY,2017,19(15):3515-3519.
APA Song, Lei.,Zheng, Mingyuan.,Pang, Jifeng.,Sebastian, Joby.,Wang, Wentao.,...&Zhang, Tao.(2017).One-pot synthesis of 2-hydroxymethyl-5-methylpyrazine from renewable 1,3-dihydroxyacetone.GREEN CHEMISTRY,19(15),3515-3519.
MLA Song, Lei,et al."One-pot synthesis of 2-hydroxymethyl-5-methylpyrazine from renewable 1,3-dihydroxyacetone".GREEN CHEMISTRY 19.15(2017):3515-3519.
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