DICP OpenIR
Synthesis and Characterization of Hydrazide-Linked and Amide Linked Organic Polymers
Liu, Zhongshan1,2; Ou, Junjie1; Wang, Hongwei1; You, Xin1,2; Ye, Mingliang1
关键词Hydrazide Amide Porous Organic Polymer Hollow Structure Enrichment Of Glycopeptide
刊名ACS Applied Materials & Interfaces
2016-11-23
DOI10.1021/acsami.6b11572
8期:46页:32060-32067
收录类别SCI
文章类型Article
WOS标题词Science & Technology ; Technology
类目[WOS]Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
关键词[WOS]SOLID-PHASE EXTRACTION ; INTERACTION LIQUID-CHROMATOGRAPHY ; INTRINSIC MICROPOROSITY PIMS ; MAGNETIC NANOPARTICLES ; STATIONARY-PHASE ; HYDROGEN STORAGE ; ROOM-TEMPERATURE ; CO2 CAPTURE ; FRAMEWORKS ; GLYCOPEPTIDES
英文摘要Four kinds of either hydrazide-linked or amide-linked polymers were facilely synthesized by using hydrazine, tetrakis(4-aminophenyl)methane (TAPM), terephthaloyl chloride (TPC), and trimesoyl chloride (TMC) as building blocks. The morphology, porosity, composition, and surface property of polymers were characterized by scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption-measurement, C-13/CP-MAS NMR, X-ray photoelectron spectroscopy, etc. The results indicated that building blocks had important effects on morphology and porosity. Poly(TMC-TAPM) synthesized with TMC and TAPM showed the highest surface area of 241.9 m(2) g(-1). In addition, note that a hollow structure with similar to 20 run wall thickness was formed in poly(TMC hydrazine) prepared with TMC and hydrazine. Further study indicated that both carboxyl groups (-COOH) and hydrazide groups (-CONH-NH2) existed on the surface of poly(TMC-hydrazine), besides the mainly hydrazide linkage (-CONH-NHOC-). Taking advantages of good hydrophilicity and special functional groups on the surface, we finally adopted poly(TMC hydrazine) to enrich glycopeptides from tryptic digest via both hydrophilic interaction chromatography method with identification of 369 unique N-glycosylation sites and hydrazide chemistry method with identification of 88 unique N-glycosylation sites, respectively.
语种英语
WOS记录号WOS:000388913900068
引用统计
被引频次:6[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/150437
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714
Liu, Zhongshan,Ou, Junjie,Wang, Hongwei,et al. Synthesis and Characterization of Hydrazide-Linked and Amide Linked Organic Polymers[J]. ACS Applied Materials & Interfaces,2016,8(46):32060-32067.
APA Liu, Zhongshan,Ou, Junjie,Wang, Hongwei,You, Xin,&Ye, Mingliang.(2016).Synthesis and Characterization of Hydrazide-Linked and Amide Linked Organic Polymers.ACS Applied Materials & Interfaces,8(46),32060-32067.
MLA Liu, Zhongshan,et al."Synthesis and Characterization of Hydrazide-Linked and Amide Linked Organic Polymers".ACS Applied Materials & Interfaces 8.46(2016):32060-32067.
条目包含的文件
条目无相关文件。
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[Liu, Zhongshan]的文章
[Ou, Junjie]的文章
[Wang, Hongwei]的文章
百度学术
百度学术中相似的文章
[Liu, Zhongshan]的文章
[Ou, Junjie]的文章
[Wang, Hongwei]的文章
必应学术
必应学术中相似的文章
[Liu, Zhongshan]的文章
[Ou, Junjie]的文章
[Wang, Hongwei]的文章
相关权益政策
暂无数据
收藏/分享
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。