DICP OpenIR
Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route
Wei, Pengfei1,2; Zhu, Xiangxue1; Wang, Yanan1,2; Chu, Weifeng1,2; Xie, Sujuan1; Yang, Zhiqiang3; Liu, Xuebin3; Li, Xiujie1; Xu, Longya1
Corresponding AuthorLi, Xiujie(xiujieli@dicp.ac.cn) ; Xu, Longya(lyxu@dicp.ac.cn)
KeywordFerrierite Microwave Zeolite synthesis Crystallization
Source PublicationMICROPOROUS AND MESOPOROUS MATERIALS
2019-05-01
ISSN1387-1811
DOI10.1016/j.micromeso.2018.12.036
Volume279Pages:220-227
Funding ProjectNational Natural Science Foundation of China[21773233] ; National Natural Science Foundation of China[21376235] ; Natural Science Foundation of Liaoning Province[201602740] ; BP Energy Innovation Laboratory
Funding OrganizationNational Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory
WOS SubjectChemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Science & Technology - Other Topics ; Materials Science
WOS KeywordSKELETAL ISOMERIZATION ; HYDROTHERMAL SYNTHESIS ; ORGANOTEMPLATE-FREE ; BETA-ZEOLITE ; FER ZEOLITE ; 1-BUTENE ; SYSTEM
AbstractFerrierite (FER) zeolite has been successfully synthesized within 2-3 h through microwave assisted crystallization without using organic structure directing agent. Crystallization temperature and seed content were found to be two of the key factors. XRD patterns and SEM images of the samples taken at different periods of time revealed that seeds were only partially dissolved during the crystallization process and silicate (alumino) species in the gel grew upon the surface of the partially dissolved seed. A core-shell zeolite growth model was proposed. Compared with original seed zeolite, as-synthesized FER zeolite had more regular morphology and larger particle size. The FER crystal size could be controlled in the range of 0.4-3.0 mu m by adjusting the particle size of the seeds. FER obtained through microwave assisted rapid synthesis showed similar catalytic performance in 1-butene skeletal isomerization with the FER obtained through conventional hydrothermal synthesis.
Language英语
Funding OrganizationNational Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Natural Science Foundation of Liaoning Province ; Natural Science Foundation of Liaoning Province ; BP Energy Innovation Laboratory ; BP Energy Innovation Laboratory
WOS IDWOS:000460843500025
PublisherELSEVIER SCIENCE BV
Citation statistics
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/165889
Collection中国科学院大连化学物理研究所
Corresponding AuthorLi, Xiujie; Xu, Longya
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, 457 Zhongshan Rd, Dalian 116023, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
3.BP China Dalian Off, Energy Innovat Lab, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Wei, Pengfei,Zhu, Xiangxue,Wang, Yanan,et al. Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2019,279:220-227.
APA Wei, Pengfei.,Zhu, Xiangxue.,Wang, Yanan.,Chu, Weifeng.,Xie, Sujuan.,...&Xu, Longya.(2019).Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route.MICROPOROUS AND MESOPOROUS MATERIALS,279,220-227.
MLA Wei, Pengfei,et al."Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route".MICROPOROUS AND MESOPOROUS MATERIALS 279(2019):220-227.
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