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Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles
Yao, Siyu1; Yang, Ce1,2; Zhao, Huabo1; Li, Siwei1; Lin, Lili1; Wen, Wen3; Liu, Jinxun4,5; Hu, Gang6; Li, Weixue4,5; Hou, Yanglong2; Ma, Ding1
Source PublicationJOURNAL OF PHYSICAL CHEMISTRY C
2017-03-09
ISSN1932-7447
DOI10.1021/acs.jpcc.7b00198
Volume121Issue:9Pages:5154-5160
Indexed BySCI
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Science & Technology - Other Topics ; Materials Science
WOS KeywordFISCHER-TROPSCH SYNTHESIS ; IRON CARBIDE NANOPARTICLES ; MINIMUM ENERGY PATHS ; ELASTIC BAND METHOD ; X-RAY-SCATTERING ; HYDROTHERMAL CONDITIONS ; SYNCHROTRON-RADIATION ; NANOCOMPOSITE MAGNETS ; COBALT NANOPARTICLES ; GRAPHITIC LAYERS
AbstractWet chemical synthesis (WCS), especially under high temperatures, is one of the most frequently used strategies for nanostructured material construction, which has been used extensively in medical-, energy-, and environment-related applications. Although knowledge about the WCS process has been accumulated in the past two decades, the high temperature used in the process and multiphase nature of intermediates and products are key factors preventing the processes from rationalization. In this paper, by using multilevel in situ cells, we developed a strategy to monitor the reaction details of WCS processed in the solid, liquid, and gas phase simultaneously. This protocol has proven successful to reconstruct the WCS process of Fe5C2 nanoparticles (NPs) and unravel the complicated chemistry in the synthesis process.
Language英语
WOS IDWOS:000396295800041
PublisherAMER CHEMICAL SOC
Citation statistics
Cited Times:9[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/169415
Collection中国科学院大连化学物理研究所
Corresponding AuthorHou, Yanglong; Ma, Ding
Affiliation1.Peking Univ, Coll Chem & Mol Engn, Beijing 100871, Peoples R China
2.Peking Univ, Coll Engn, Beijing 100871, Peoples R China
3.Chinese Acad Sci, Shanghai Inst Appl Phys, SSRF, Shanghai 201204, Peoples R China
4.Univ Sci & Technol China, Dept Chem Phys, Hefei 230026, Peoples R China
5.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
6.Israel Chem Ltd, Shanghai 200021, Peoples R China
Recommended Citation
GB/T 7714
Yao, Siyu,Yang, Ce,Zhao, Huabo,et al. Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles[J]. JOURNAL OF PHYSICAL CHEMISTRY C,2017,121(9):5154-5160.
APA Yao, Siyu.,Yang, Ce.,Zhao, Huabo.,Li, Siwei.,Lin, Lili.,...&Ma, Ding.(2017).Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles.JOURNAL OF PHYSICAL CHEMISTRY C,121(9),5154-5160.
MLA Yao, Siyu,et al."Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles".JOURNAL OF PHYSICAL CHEMISTRY C 121.9(2017):5154-5160.
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