DICP OpenIR
Microfluidic Synthesis of UiO-66 Metal-organic Frameworks Modified with Different Functional Groups
Sheng Bingchen1; Li Cong1; Liu Yingya1; Wang Anjie1; Wang Yao1; Zhang Jian2; Liu Weixu1
Corresponding AuthorWang Yao(wangyao@dlut.edu.cn)
KeywordMetal-organic framework UiO-66 Nanomaterial Microfluidic synthesis
Source PublicationCHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
2019-07-10
ISSN0251-0790
DOI10.7503/cjcu20180831
Volume40Issue:7Pages:1365-1373
Funding ProjectNational Key R&D Program of China[2016YFE0109800] ; National Natural Science Foundation of China[21473017] ; National Natural Science Foundation of China[21373215] ; Fundamental Research Funds for the Central Universities, China[DUT17JC20] ; Open Project of the State Key Laboratory of Fine Chemicals, China[KF1405]
Funding OrganizationNational Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China
WOS SubjectChemistry, Multidisciplinary
WOS Research AreaChemistry
WOS KeywordSIZE ; DESIGN ; FLOW
AbstractZirconium based metal-organic framework UiO-66 was synthesized continuously by microfluidic method. Compared with the traditional solvothermal synthesis in batch reactors, microfluidic synthesis is more efficient. It has the advantages in highly efficient mixing and heat transfer, thus lead to enhanced reaction rates. Microfluidic synthesis can obtain uniform hexahedral crystalline products in nanometer range(less than 100 nm). The influences of temperature, total flowrate and residence time on the obtained products were investigated. Higher temperature benefited the growth of crystal. When flowrate increased, crystal sizes of UiO-66 synthesized by microfluidic method decreased. Crystal growth required sufficient residence time (20 min), but if the residence time was prolonged further, the crystal particle size would not change any more. By optimizing the synthetic parameters, UiO-66 modified with different functional groups, UiO-66-X (X = NH2, NO2, Br), could be synthesized continuously by microfluidic synthesis.
Language英语
Funding OrganizationNational Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; National Key R&D Program of China ; National Key R&D Program of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Fundamental Research Funds for the Central Universities, China ; Fundamental Research Funds for the Central Universities, China ; Open Project of the State Key Laboratory of Fine Chemicals, China ; Open Project of the State Key Laboratory of Fine Chemicals, China
WOS IDWOS:000490720100005
PublisherHIGHER EDUCATION PRESS
Citation statistics
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/172395
Collection中国科学院大连化学物理研究所
Corresponding AuthorWang Yao
Affiliation1.Dalian Univ Technol, Sch Chem Engn, Dalian 116024, Peoples R China
2.Chinese Acad Sci, Lab Catalysts & New Mat, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Sheng Bingchen,Li Cong,Liu Yingya,et al. Microfluidic Synthesis of UiO-66 Metal-organic Frameworks Modified with Different Functional Groups[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2019,40(7):1365-1373.
APA Sheng Bingchen.,Li Cong.,Liu Yingya.,Wang Anjie.,Wang Yao.,...&Liu Weixu.(2019).Microfluidic Synthesis of UiO-66 Metal-organic Frameworks Modified with Different Functional Groups.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,40(7),1365-1373.
MLA Sheng Bingchen,et al."Microfluidic Synthesis of UiO-66 Metal-organic Frameworks Modified with Different Functional Groups".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 40.7(2019):1365-1373.
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