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题名: Template-assisted syntheses of two novel porous zirconium methylphosphonates
作者: Wu, ZB;  Liu, ZM;  Tian, P;  He, YL;  Xu, L;  Yang, Y;  Zhang, YY;  Bao, XH;  Liu, XM;  Liu, XC
通讯作者: 刘中民
关键词: porous zirconium methylphosphonate ;  template-assisted synthesis ;  dibutyl methylphosphonate
刊名: MICROPOROUS AND MESOPOROUS MATERIALS
发表日期: 2005-06-06
DOI: 10.1016/j.micromeso.2005.01.031
卷: 81, 期:1-3, 页:175-183
收录类别: SCI
文章类型: Article
部门归属: 8,5
项目归属: 803,502
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences ;  Technology
类目[WOS]: Chemistry, Applied ;  Chemistry, Physical ;  Nanoscience & Nanotechnology ;  Materials Science, Multidisciplinary
研究领域[WOS]: Chemistry ;  Science & Technology - Other Topics ;  Materials Science
英文摘要: Two porous zirconium methylphosphonates (designated as ZMPmi and ZMPme respectively) were synthesized by using dibutyl methylphosphonate (DBMP) as a template. Two efficient post-synthetic treatments were developed to remove the incorporated template without destroying the hybrid structures. The materials were characterized by SEM, EPMA, TG, DTA, FTIR, and NMR. Specific surface area and porosity were evaluated by BET, alpha(s)-plots and DFT methods based on N-2 adsorption-desorption isotherms. The specific surface areas of ZMPmi and ZMPme are determined to be 279 and 403 m(2) g(-1) and the maxima of pore size distributions are at 0.7 and 1.3 nm respectively. (c) 2005 Elsevier Inc. All rights reserved.
关键词[WOS]: ALUMINUM METHYLPHOSPHONATE ;  UNIDIMENSIONAL CHANNELS ;  PHOSPHONATE MATERIALS ;  MESOPOROUS MATERIALS ;  CRYSTAL-STRUCTURES ;  EXTRACTION ;  FRAMEWORK
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000229665200021
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/80947
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China

Recommended Citation:
Wu, ZB,Liu, ZM,Tian, P,et al. Template-assisted syntheses of two novel porous zirconium methylphosphonates[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2005,81(1-3):175-183.
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