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Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography
Shu, X; Chen, LX; Yang, BC; Guan, YF
关键词Monolithic Column Butyl Methacrylate Phase Stationary Phases Lc
刊名JOURNAL OF CHROMATOGRAPHY A
2004-10-15
DOI10.1016/j.chroma.2004.08.009
1052期:1-2页:205-209
收录类别SCI
文章类型Article
项目归属105
产权排名1;1
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]ROD COLUMNS ; ELECTROCHROMATOGRAPHY
英文摘要Long methacrylate monolithic columns (100 cm x 320 mum i.d.) were prepared from silanized fused-silica capillaries of 320 mum i.d. by in situ copolymerization of butyl methacrylate (BMA) with ethylene dimethacrylate (EDMA) in the presence of a suitable porogen. The separation performance and selectivity of the column were evaluated and compared with a 25 cm x 320 mum i.d. column prepared in the same way by capillary high-performance liquid chromatography (mu-HPLC) The results showed that the 1 m long monolithic column can generate 33 x 10(3) plate number and exhibited good permeability, higher sample loadability, and separation capability. (C) 2004 Elsevier B.V. All rights reserved.
语种英语
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WOS记录号WOS:000224501000025
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被引频次:21[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/81703
专题中国科学院大连化学物理研究所
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Dept Analyt Chem & Micro Instrumentat, Dalian 116012, Peoples R China
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GB/T 7714
Shu, X,Chen, LX,Yang, BC,et al. Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2004,1052(1-2):205-209.
APA Shu, X,Chen, LX,Yang, BC,&Guan, YF.(2004).Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography.JOURNAL OF CHROMATOGRAPHY A,1052(1-2),205-209.
MLA Shu, X,et al."Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography".JOURNAL OF CHROMATOGRAPHY A 1052.1-2(2004):205-209.
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