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题名: Hydrothermal synthesis and characterization of microporous crystals of trivalent metal-containing zirconium phosphates
作者: Sun, ZG;  Liu, ZM;  Xu, L;  Yang, Y;  He, YL
关键词: hydrothermal synthesis ;  zirconium phosphates ;  (P-31, Al-27) MAS NMR
刊名: CATALYSIS TODAY
发表日期: 2004-09-01
DOI: 10.1016/j.cattod.2004.06.022
卷: 93-5, 期:93-95, 页:639-643
收录类别: SCI ;  ISTP
文章类型: Article
项目归属: 803
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences ;  Technology
类目[WOS]: Chemistry, Applied ;  Chemistry, Physical ;  Engineering, Chemical
研究领域[WOS]: Chemistry ;  Engineering
英文摘要: Two organically templated trivalent metal-containing crystalline zirconium phosphate materials FeZrPO-8 and AlZrPO-8 have been prepared hydrothermally by using fluoride as a mineralizer, and 1,6-diaminohexane (DAH) as templates. The powder XRD patterns indicate that the as-synthesized products are new materials. Substitutions of Al3+ or Fe3+ into Zr4+ sites were confirmed by a combination of powder X-ray diffraction (XRD) and nuclear magnetic resonance (NMR) studies. The thermal behavior of the title compounds have been investigated using TG-DTA and X-ray thermodiffractometry, which indicated that the inorganic framework of the compounds are thermally stable up to similar to400 degreesC. (C) 2004 Elsevier B.V. All rights reserved.
关键词[WOS]: P-31 NMR ;  TITANIUM PHOSPHATES ;  OPEN-FRAMEWORK ;  X-RAY ;  ETHYLENEDIAMINE ;  CONDUCTORS ;  FLUORIDES ;  AL-27
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000223973200091
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/81813
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dept Nat Gas Chem & Appl Catalysis, Dalian 116023, Peoples R China
2.Liaoning Normal Univ, Dept Chem, Dalian 116029, Peoples R China

Recommended Citation:
Sun, ZG,Liu, ZM,Xu, L,et al. Hydrothermal synthesis and characterization of microporous crystals of trivalent metal-containing zirconium phosphates[J]. CATALYSIS TODAY,2004,93-5(93-95):639-643.
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