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Synthesis and spectroscopic study of mesoporous aluminum methylphosphonate foam templated by dibutyl methylphosphonate
Wu, ZB; Liu, ZM; Tian, P; He, YL; Xu, L; Liu, XM; Bao, XH; Liu, XC
关键词Aluminum Methylphosphonate Dibutyl Methylphosphonate Foam Mesoporous Template
刊名MICROPOROUS AND MESOPOROUS MATERIALS
2003-08-14
DOI10.1016/S1387-1811(03)00393-7
62期:1-2页:61-71
收录类别SCI
文章类型Article
部门归属803
项目归属803
产权排名1;1
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Applied ; Chemistry, Physical ; Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
研究领域[WOS]Chemistry ; Science & Technology - Other Topics ; Materials Science
关键词[WOS]LINED UNIDIMENSIONAL CHANNELS ; METAL-ORGANIC FRAMEWORK ; ALMEPO-ALPHA ; DIMETHYL METHYLPHOSPHONATE ; CO-CONDENSATION ; HYBRID ; SILICA ; MCM-41 ; BETA ; TRANSFORMATION
英文摘要New types of templates and novel interactive mechanisms between template and framework are very important for creating porous materials. In this work, by using neutral dibutyl methylphosphonate as a template, an inorganic-organic hybrid mesoporous material, aluminum methylphosphonate, was prepared. The as-synthesized material was studied by P-31 magnetic angle spinning nuclear magnetic resonance (MAS NMR), Al-27 MAS NMR, C-13 CP/MAS, FT-IR spectroscopy, thermogravimetry (TG), differential thermal analysis (DTA), and transmission electron microscopy. After thermal treatment at 673 K and 10 mmHg for 2 h, hybrid mesoporous foam was obtained. The transformation process was investigated by FT-IR. TG-DTA results indicate that the methyl group bonded to the framework keeps intact up to 792 K under air and 823 K under nitrogen. The characterization results from nitrogen gas adsorption-desorption measurements show that the BET surface area and the Barrett-Joyner-Halenda desorption cumulative pore volume of the foam are 90 m(2) g(-1) and 0.32 cm(3) g(-1) respectively. (C) 2003 Elsevier Inc. All rights reserved.
语种英语
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WOS记录号WOS:000184626000006
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被引频次:6[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/83027
专题中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
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GB/T 7714
Wu, ZB,Liu, ZM,Tian, P,et al. Synthesis and spectroscopic study of mesoporous aluminum methylphosphonate foam templated by dibutyl methylphosphonate[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2003,62(1-2):61-71.
APA Wu, ZB.,Liu, ZM.,Tian, P.,He, YL.,Xu, L.,...&Liu, XC.(2003).Synthesis and spectroscopic study of mesoporous aluminum methylphosphonate foam templated by dibutyl methylphosphonate.MICROPOROUS AND MESOPOROUS MATERIALS,62(1-2),61-71.
MLA Wu, ZB,et al."Synthesis and spectroscopic study of mesoporous aluminum methylphosphonate foam templated by dibutyl methylphosphonate".MICROPOROUS AND MESOPOROUS MATERIALS 62.1-2(2003):61-71.
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