DICP OpenIR
Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry
Zhu, SK; Lu, X; Dong, L; Xing, J; Su, XL; Kong, HW; Xu, GW; Wu, CY; Wu CY(吴采樱); Wu CY(吴采樱)
KeywordComprehensive Two-dimensional Gas Chromatography Time-of-flight Mass Spectrometry Gas Chromatography-mass Spectrometry Multiple Internal Standards Calibration Essential Oils Tobacco
Source PublicationJOURNAL OF CHROMATOGRAPHY A
2005-09-09
DOI10.1016/j.chroma.2005.04.007
Volume1086Issue:1-2Pages:107-114
Indexed ByISTP ; SCI
SubtypeArticle
Department18
Funding Project1808
Contribution Rank2;2
WOS HeadingsScience & Technology ; Life Sciences & Biomedicine ; Physical Sciences
WOS SubjectBiochemical Research Methods ; Chemistry, Analytical
WOS Research AreaBiochemistry & Molecular Biology ; Chemistry
WOS KeywordCIGARETTE-SMOKE
AbstractA quantitative analysis of the individual compounds in tobacco essential oils is performed by comprehensive two-dimensional gas chromatography (GC x GC) combined with flame ionization detector (FID). A time-of-flight mass spectrometer (TOF/MS) was coupled to GC x GC for the identification of the resolved peaks. The response of a flame ionization detector to different compound classes was calibrated using multiple internal standards. In total, 172 compounds were identified with good match and 61 compounds with high probability value were reliably quantified. For comparative purposes, the essential oil sample was also quantified by one-dimensional gas chromatography-mass spectrometry (GC/MS) with multiple internal standards method. The results showed that there was close agreement between the two analysis methods when the peak purity and match quality in one-dimensional GC/MS are high enough. (c) 2005 Elsevier B.V. All rights reserved.
Language英语
URL查看原文
WOS IDWOS:000231185500012
Citation statistics
Cited Times:41[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/92903
Collection中国科学院大连化学物理研究所
Corresponding AuthorWu CY(吴采樱); Wu CY(吴采樱)
Affiliation1.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China
2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China
Recommended Citation
GB/T 7714
Zhu, SK,Lu, X,Dong, L,et al. Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry[J]. JOURNAL OF CHROMATOGRAPHY A,2005,1086(1-2):107-114.
APA Zhu, SK.,Lu, X.,Dong, L.,Xing, J.,Su, XL.,...&吴采樱.(2005).Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry.JOURNAL OF CHROMATOGRAPHY A,1086(1-2),107-114.
MLA Zhu, SK,et al."Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry".JOURNAL OF CHROMATOGRAPHY A 1086.1-2(2005):107-114.
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