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Template-assisted syntheses of porous metal methylphosphonates
Wu, ZB; Tian, JC; Liu, ZM; Tian, P; Xu, L; Yang, Y; Zhang, YY; Bao, XH; Liu, XM; Liu, XC; Liu ZM(刘中民); Liu ZM(刘中民)
KeywordDibutyl Methylphosphonate Template-assisted Synthesis Porous Material Metal Methylphosphonate
Source PublicationJOURNAL OF POROUS MATERIALS
2006
DOI10.1007/s10934-006-5492-4
Volume13Issue:1Pages:73-80
Indexed BySCI
SubtypeArticle
Department8,5
Funding Project803,502
Contribution Rank1;1
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Applied ; Chemistry, Physical ; Materials Science, Multidisciplinary
WOS Research AreaChemistry ; Materials Science
WOS KeywordCARBON MOLECULAR-SIEVES ; DIMETHYL METHYLPHOSPHONATE ; ORGANIC TEMPLATES ; SILICA ; OXIDES ; ADSORPTION ; DESIGN ; IR
AbstractNeutral dibutyl methylphosphonate (DBMP) is used as a template to prepare porous metal methylphosphonates (metal = aluminum, titanium, zirconium). The removal of DBMP in the as-synthesized materials could be easily achieved by evaporation under vacuum without destroying the hybrid structure, as evidenced by elemental analyses, FT-IR spectra, C-13 CP/MAS NMR and nitrogen adsorption-desorption isotherms. Thermal analyses show that three porous hybrid samples have high thermal stability in air. The exothermic weight losses due to oxidation combustion of organic species occluded in samples appear after 730 K. Furthermore, the templating effect of DBMP is also confirmed by comparing the hybrid materials synthesized in the presence or the absence of the template.
Language英语
URL查看原文
WOS IDWOS:000235808000009
Citation statistics
Cited Times:6[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/93681
Collection中国科学院大连化学物理研究所
Corresponding AuthorLiu ZM(刘中民); Liu ZM(刘中民)
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China
2.Jiaozuo Univ, Dept Biochem & Environm Engn, Jiaozuo 454003, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
Recommended Citation
GB/T 7714
Wu, ZB,Tian, JC,Liu, ZM,et al. Template-assisted syntheses of porous metal methylphosphonates[J]. JOURNAL OF POROUS MATERIALS,2006,13(1):73-80.
APA Wu, ZB.,Tian, JC.,Liu, ZM.,Tian, P.,Xu, L.,...&刘中民.(2006).Template-assisted syntheses of porous metal methylphosphonates.JOURNAL OF POROUS MATERIALS,13(1),73-80.
MLA Wu, ZB,et al."Template-assisted syntheses of porous metal methylphosphonates".JOURNAL OF POROUS MATERIALS 13.1(2006):73-80.
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