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题名: Template-assisted syntheses of porous metal methylphosphonates
作者: Wu, ZB;  Tian, JC;  Liu, ZM;  Tian, P;  Xu, L;  Yang, Y;  Zhang, YY;  Bao, XH;  Liu, XM;  Liu, XC
通讯作者: 刘中民
关键词: dibutyl methylphosphonate ;  template-assisted synthesis ;  porous material ;  metal methylphosphonate
刊名: JOURNAL OF POROUS MATERIALS
发表日期: 2006
DOI: 10.1007/s10934-006-5492-4
卷: 13, 期:1, 页:73-80
收录类别: SCI
文章类型: Article
部门归属: 8,5
项目归属: 803,502
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences ;  Technology
类目[WOS]: Chemistry, Applied ;  Chemistry, Physical ;  Materials Science, Multidisciplinary
研究领域[WOS]: Chemistry ;  Materials Science
英文摘要: Neutral dibutyl methylphosphonate (DBMP) is used as a template to prepare porous metal methylphosphonates (metal = aluminum, titanium, zirconium). The removal of DBMP in the as-synthesized materials could be easily achieved by evaporation under vacuum without destroying the hybrid structure, as evidenced by elemental analyses, FT-IR spectra, C-13 CP/MAS NMR and nitrogen adsorption-desorption isotherms. Thermal analyses show that three porous hybrid samples have high thermal stability in air. The exothermic weight losses due to oxidation combustion of organic species occluded in samples appear after 730 K. Furthermore, the templating effect of DBMP is also confirmed by comparing the hybrid materials synthesized in the presence or the absence of the template.
关键词[WOS]: CARBON MOLECULAR-SIEVES ;  DIMETHYL METHYLPHOSPHONATE ;  ORGANIC TEMPLATES ;  SILICA ;  OXIDES ;  ADSORPTION ;  DESIGN ;  IR
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000235808000009
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/93681
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China
2.Jiaozuo Univ, Dept Biochem & Environm Engn, Jiaozuo 454003, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China

Recommended Citation:
Wu, ZB,Tian, JC,Liu, ZM,et al. Template-assisted syntheses of porous metal methylphosphonates[J]. JOURNAL OF POROUS MATERIALS,2006,13(1):73-80.
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