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Template-assisted syntheses of porous metal methylphosphonates
Wu, ZB; Tian, JC; Liu, ZM; Tian, P; Xu, L; Yang, Y; Zhang, YY; Bao, XH; Liu, XM; Liu, XC; Liu ZM(刘中民); Liu ZM(刘中民)
关键词Dibutyl Methylphosphonate Template-assisted Synthesis Porous Material Metal Methylphosphonate
刊名JOURNAL OF POROUS MATERIALS
2006
DOI10.1007/s10934-006-5492-4
13期:1页:73-80
收录类别SCI
文章类型Article
部门归属8,5
项目归属803,502
产权排名1;1
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Applied ; Chemistry, Physical ; Materials Science, Multidisciplinary
研究领域[WOS]Chemistry ; Materials Science
关键词[WOS]CARBON MOLECULAR-SIEVES ; DIMETHYL METHYLPHOSPHONATE ; ORGANIC TEMPLATES ; SILICA ; OXIDES ; ADSORPTION ; DESIGN ; IR
英文摘要Neutral dibutyl methylphosphonate (DBMP) is used as a template to prepare porous metal methylphosphonates (metal = aluminum, titanium, zirconium). The removal of DBMP in the as-synthesized materials could be easily achieved by evaporation under vacuum without destroying the hybrid structure, as evidenced by elemental analyses, FT-IR spectra, C-13 CP/MAS NMR and nitrogen adsorption-desorption isotherms. Thermal analyses show that three porous hybrid samples have high thermal stability in air. The exothermic weight losses due to oxidation combustion of organic species occluded in samples appear after 730 K. Furthermore, the templating effect of DBMP is also confirmed by comparing the hybrid materials synthesized in the presence or the absence of the template.
语种英语
原文出处查看原文
WOS记录号WOS:000235808000009
引用统计
被引频次:6[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/93681
专题中国科学院大连化学物理研究所
通讯作者Liu ZM(刘中民); Liu ZM(刘中民)
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China
2.Jiaozuo Univ, Dept Biochem & Environm Engn, Jiaozuo 454003, Peoples R China
3.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
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GB/T 7714
Wu, ZB,Tian, JC,Liu, ZM,et al. Template-assisted syntheses of porous metal methylphosphonates[J]. JOURNAL OF POROUS MATERIALS,2006,13(1):73-80.
APA Wu, ZB.,Tian, JC.,Liu, ZM.,Tian, P.,Xu, L.,...&刘中民.(2006).Template-assisted syntheses of porous metal methylphosphonates.JOURNAL OF POROUS MATERIALS,13(1),73-80.
MLA Wu, ZB,et al."Template-assisted syntheses of porous metal methylphosphonates".JOURNAL OF POROUS MATERIALS 13.1(2006):73-80.
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