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Determination of DL-tetrahydropalmatine in Corydalis yanhusuo by L-tetrahydropalmatine imprinted monolithic column coupling with reversed-phase high performance liquid chromatography
Ou, JJ; Kong, L; Pan, CS; Su, XY; Lei, XY; Zou, HF; Zou HF(邹汉法); Zou HF(邹汉法)
关键词Molecularly Imprinted Polymer Monolithic Column Tetrahydropalmatine Chiral Separation On-line Solid-phase Extraction Corydalis Yanhusuo
刊名JOURNAL OF CHROMATOGRAPHY A
2006-06-09
ISSN0021-9673
DOI10.1016/j.chroma.2006.03.084
1117期:2页:163-169
收录类别SCI
文章类型Article
部门归属18
项目归属1809
产权排名1;1
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]GROWTH-FACTOR RECEPTOR ; ENVIRONMENTAL WATER ; MASS-SPECTROMETRY ; STATIONARY PHASES ; ORGANIC MODIFIER ; EXTRACTION ; POLYMERS ; SEPARATION ; SAMPLES ; ENANTIOMERS
英文摘要A method for direct determination of DL-tetrahydropalmatine (DL-THP) in Corydalis yanhusuo, a traditional Chinese herb, by L-THP imprinted monolithic precolumn on-line/off-line coupling with reversed-phase high performance liquid chromatography (RP-HPLC) was developed. The L-THP imprinted monolithic column has been prepared by in situ polymerization using methacrylic acid (MAA) and ethylene dimethacrylate (EDMA) as functional monomer and cross-linker, respectively. With the optimization of chromatographic conditions, such as mobile phase composition, flow rate, column temperature and sample loading, for the separation of enantiomer, DL-THP was base-line separated on the MIP. The imprinted monolithic column was used as a precolumn for fractionation of the C. yanhusuo extract. Both the non-retained and retained fractions were separated by RP-HPLC. Meanwhile, the D-THP and L-THP can be detected in the non-retained and retained fractions, respectively. Additionally, direct determination of L-THP using molecularly imprinted monolith on-line coupling with a reversed-phase column was acquired. (c) 2006 Elsevier B.V. All rights reserved.
语种英语
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WOS记录号WOS:000238005800007
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被引频次:103[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/93729
专题中国科学院大连化学物理研究所
通讯作者Zou HF(邹汉法); Zou HF(邹汉法)
作者单位Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116023, Peoples R China
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Ou, JJ,Kong, L,Pan, CS,et al. Determination of DL-tetrahydropalmatine in Corydalis yanhusuo by L-tetrahydropalmatine imprinted monolithic column coupling with reversed-phase high performance liquid chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2006,1117(2):163-169.
APA Ou, JJ.,Kong, L.,Pan, CS.,Su, XY.,Lei, XY.,...&邹汉法.(2006).Determination of DL-tetrahydropalmatine in Corydalis yanhusuo by L-tetrahydropalmatine imprinted monolithic column coupling with reversed-phase high performance liquid chromatography.JOURNAL OF CHROMATOGRAPHY A,1117(2),163-169.
MLA Ou, JJ,et al."Determination of DL-tetrahydropalmatine in Corydalis yanhusuo by L-tetrahydropalmatine imprinted monolithic column coupling with reversed-phase high performance liquid chromatography".JOURNAL OF CHROMATOGRAPHY A 1117.2(2006):163-169.
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