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On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum
Zhang, Jie; Zhang, Lihua; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Hu, Yushu; Zhang, Yukui; Zhang LH(张丽华); Zhang LH(张丽华)
关键词Ganoderma Lucidum Mass Spectrometry Natural Products Supercritical Fluid Extraction
刊名JOURNAL OF SEPARATION SCIENCE
2006-11-01
DOI10.1002/jscc.200600217
29期:16页:2514-2522
收录类别SCI
文章类型Article
部门归属18
项目归属1810
产权排名1;1
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
关键词[WOS]AROMATIC-HYDROCARBONS ; QUANTITATIVE-ANALYSIS ; HPLC SYSTEM ; SEPARATION ; MATRICES ; TRIACYLGLYCEROLS ; PRODUCTS ; COLUMN
英文摘要A novel on-line system combining supercritical fluid extraction (SFE) and two-dimensional high performance liquid chromatography (2D-HPLC) was developed. A trap column and two three-port valves were employed to couple SFE and 2D-HPLC system, which was composed of a CN column and a monolithic silica column, connected by a 10-port dual-position valve. The analytes extracted by supercritical CO2 were completely transferred to the 2D-HPLC system. After separation in two orthogonal modes, the eluents were delivered to APCI-tandem-MS for identification of the samples. In this way, sample preparation, separation, detection, and identification were integrated into an on-line system permitting analysis of the fruiting bodies of Ganoderma lucidum, and at least 73 components in the extract were resolved with calculated peak capacity of up to 1643.
语种英语
原文出处查看原文
WOS记录号WOS:000242242300013
引用统计
被引频次:19[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://cas-ir.dicp.ac.cn/handle/321008/97575
专题中国科学院大连化学物理研究所
通讯作者Zhang LH(张丽华); Zhang LH(张丽华)
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian, Peoples R China
2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78285 USA
推荐引用方式
GB/T 7714
Zhang, Jie,Zhang, Lihua,Duan, Jicheng,et al. On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum[J]. JOURNAL OF SEPARATION SCIENCE,2006,29(16):2514-2522.
APA Zhang, Jie.,Zhang, Lihua.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&张丽华.(2006).On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum.JOURNAL OF SEPARATION SCIENCE,29(16),2514-2522.
MLA Zhang, Jie,et al."On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum".JOURNAL OF SEPARATION SCIENCE 29.16(2006):2514-2522.
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