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On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum
Zhang, Jie; Zhang, Lihua; Duan, Jicheng; Liang, Zhen; Zhang, Weibing; Hu, Yushu; Zhang, Yukui; Zhang LH(张丽华); Zhang LH(张丽华)
KeywordGanoderma Lucidum Mass Spectrometry Natural Products Supercritical Fluid Extraction
Source PublicationJOURNAL OF SEPARATION SCIENCE
2006-11-01
DOI10.1002/jscc.200600217
Volume29Issue:16Pages:2514-2522
Indexed BySCI
SubtypeArticle
Department18
Funding Project1810
Contribution Rank1;1
WOS HeadingsScience & Technology ; Physical Sciences
WOS SubjectChemistry, Analytical
WOS Research AreaChemistry
WOS KeywordAROMATIC-HYDROCARBONS ; QUANTITATIVE-ANALYSIS ; HPLC SYSTEM ; SEPARATION ; MATRICES ; TRIACYLGLYCEROLS ; PRODUCTS ; COLUMN
AbstractA novel on-line system combining supercritical fluid extraction (SFE) and two-dimensional high performance liquid chromatography (2D-HPLC) was developed. A trap column and two three-port valves were employed to couple SFE and 2D-HPLC system, which was composed of a CN column and a monolithic silica column, connected by a 10-port dual-position valve. The analytes extracted by supercritical CO2 were completely transferred to the 2D-HPLC system. After separation in two orthogonal modes, the eluents were delivered to APCI-tandem-MS for identification of the samples. In this way, sample preparation, separation, detection, and identification were integrated into an on-line system permitting analysis of the fruiting bodies of Ganoderma lucidum, and at least 73 components in the extract were resolved with calculated peak capacity of up to 1643.
Language英语
URL查看原文
WOS IDWOS:000242242300013
Citation statistics
Cited Times:21[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/97575
Collection中国科学院大连化学物理研究所
Corresponding AuthorZhang LH(张丽华); Zhang LH(张丽华)
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian, Peoples R China
2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78285 USA
Recommended Citation
GB/T 7714
Zhang, Jie,Zhang, Lihua,Duan, Jicheng,et al. On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum[J]. JOURNAL OF SEPARATION SCIENCE,2006,29(16):2514-2522.
APA Zhang, Jie.,Zhang, Lihua.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&张丽华.(2006).On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum.JOURNAL OF SEPARATION SCIENCE,29(16),2514-2522.
MLA Zhang, Jie,et al."On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum".JOURNAL OF SEPARATION SCIENCE 29.16(2006):2514-2522.
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