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Rapid characterization of the sucrose esters from oriental tobacco using liquid chromatography/ion trap mass spectrometry
Ding, Li; Xie, Fuwei; Zhao, Mingyue; Xie, Jianping; Xu, Guowang; Xu GW(许国旺); Xu GW(许国旺)
Source PublicationRAPID COMMUNICATIONS IN MASS SPECTROMETRY
2006
DOI10.1002/rcm.2664
Volume20Issue:19Pages:2816-2822
Indexed BySCI
SubtypeArticle
Department18
Funding Project1808
Contribution Rank1;1
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS SubjectChemistry, Analytical ; Spectroscopy
WOS Research AreaChemistry ; Spectroscopy
WOS KeywordTAXUS-WALLICHIANA ; COMPONENTS ; TAXOIDS ; LEAF
AbstractSucrose esters (SEs) from oriental tobacco are normally characterized by gas chromatography/mass spectrometry (GC/MS) after a long saponification and derivatization procedure. To simplify the process, a rapid method has been developed by using liquid chromatography coupled with electrospray ion trap mass spectrometry (LC/ESI-MSn). Using the characteristic fragmentation behavior of abundant SEs identified by GC/MS after purification by gel permeation chromatography (GPC) from cuticular waxes of green oriental tobacco leaf, two types of SEs from green and cured oriental tobacco were identified by MSn analysis. The first is one of three types reported formerly and has 13 SE homologues. However, the presence of unsaturation in one of the acyl substituents of this first type gave rise. to a new series with three homologues. The other was found to be a new type and had three homologues. The proposed method enables the rapid and sensitive characterization of SEs from oriental tobacco. Copyright (c) 2006 John Wiley & Sons, Ltd.
Language英语
URL查看原文
WOS IDWOS:000241040400004
Citation statistics
Cited Times:11[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://cas-ir.dicp.ac.cn/handle/321008/97607
Collection中国科学院大连化学物理研究所
Corresponding AuthorXu GW(许国旺); Xu GW(许国旺)
Affiliation1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116023, Peoples R China
2.CNTC, Zhengzhou Tobacco Res Inst, Dept Chem, Zhengzhou 450001, Peoples R China
Recommended Citation
GB/T 7714
Ding, Li,Xie, Fuwei,Zhao, Mingyue,et al. Rapid characterization of the sucrose esters from oriental tobacco using liquid chromatography/ion trap mass spectrometry[J]. RAPID COMMUNICATIONS IN MASS SPECTROMETRY,2006,20(19):2816-2822.
APA Ding, Li.,Xie, Fuwei.,Zhao, Mingyue.,Xie, Jianping.,Xu, Guowang.,...&许国旺.(2006).Rapid characterization of the sucrose esters from oriental tobacco using liquid chromatography/ion trap mass spectrometry.RAPID COMMUNICATIONS IN MASS SPECTROMETRY,20(19),2816-2822.
MLA Ding, Li,et al."Rapid characterization of the sucrose esters from oriental tobacco using liquid chromatography/ion trap mass spectrometry".RAPID COMMUNICATIONS IN MASS SPECTROMETRY 20.19(2006):2816-2822.
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