中国科学院大连化学物理研究所机构知识库
Advanced  
DICP OpenIR  > 中国科学院大连化学物理研究所  > 期刊论文
题名: On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample
作者: Zhang, Xiuli;  Martens, Dieter;  Kraemer, Petra M.;  Kettrup, Antonius A.;  Liang, Xinmiao
通讯作者: 梁鑫淼
关键词: immunoaffinity column ;  diuron ;  on-line ;  LC-MS-MS ;  matrix effect ;  wastewater
刊名: JOURNAL OF CHROMATOGRAPHY A
发表日期: 2006-11-10
DOI: 10.1016/j.chroma.2006.08.007
卷: 1133, 期:1-2, 页:112-118
收录类别: SCI
文章类型: Article
部门归属: 18
项目归属: 1803
产权排名: 1;1
WOS标题词: Science & Technology ;  Life Sciences & Biomedicine ;  Physical Sciences
类目[WOS]: Biochemical Research Methods ;  Chemistry, Analytical
研究领域[WOS]: Biochemistry & Molecular Biology ;  Chemistry
英文摘要: An on-line immunoaffinity column with liquid chromatography/tandem mass spectrometry (IAC-LC-MS/MS) method for the determination of diuron in water matrices was described. This method used a sol-gel immunoaffinity column (20 mm x 4 mm I.D.) for on-line sample cleanup and enrichment, a monolithic analytical column (100 mm x 4.6 mm I.D.) for separation, and a triple quadrupole mass spectrometer for quantitation. The major challenges for the on-line set-up were discussed. The optimized on-line protocol was emphasized by the fact that low limit of quantitation (LOQ) of 1.0 ng/L was achieved with only 2.5-mL sample. In addition, a satisfactory accuracy (similar to 90% of recovery) and precision (< 6% of relative standard deviation) at 50 ng/L concentration were also obtained. Due to the ability of the sol-gel immunoaffinity column to eliminate matrix effect, the on-line IAC-LC-MS/MS analysis method can reliably determine diuron in wastewater treatment plant effluent sample. (c) 2006 Elsevier B.V. All rights reserved.
关键词[WOS]: SOLID-PHASE EXTRACTION ;  PESTICIDE-RESIDUES ;  TRANSFORMATION PRODUCTS ;  EMERGING CONTAMINANTS ;  ENDOCRINE DISRUPTORS ;  LEVEL DETERMINATION ;  GAS-CHROMATOGRAPHY ;  CURRENT ISSUES ;  SURFACE-WATER ;  S-TRIAZINES
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000241772800014
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/97791
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

Files in This Item:

There are no files associated with this item.


作者单位: 1.LUFA Speyer, D-67346 Speyer, Germany
2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
3.GSF, Inst Ecol Chem, Natl Res Ctr Environm & Hlth, D-85764 Neuherberg, Germany
4.Tech Univ Munich, Lehrstuhl Okol Chem & Umweltanalyt, D-85350 Freising Weihenstephan, Germany

Recommended Citation:
Zhang, Xiuli,Martens, Dieter,Kraemer, Petra M.,et al. On-line immunoaffinity column-liquid chromatography-tandem mass spectrometry method for trace analysis of diuron in wastewater treatment plant effluent sample[J]. JOURNAL OF CHROMATOGRAPHY A,2006,1133(1-2):112-118.
Service
 Recommend this item
 Sava as my favorate item
 Show this item's statistics
 Export Endnote File
Google Scholar
 Similar articles in Google Scholar
 [Zhang, Xiuli]'s Articles
 [Martens, Dieter]'s Articles
 [Kraemer, Petra M.]'s Articles
CSDL cross search
 Similar articles in CSDL Cross Search
 [Zhang, Xiuli]‘s Articles
 [Martens, Dieter]‘s Articles
 [Kraemer, Petra M.]‘s Articles
Related Copyright Policies
Null
Social Bookmarking
  Add to CiteULike  Add to Connotea  Add to Del.icio.us  Add to Digg  Add to Reddit 
所有评论 (0)
暂无评论
 
评注功能仅针对注册用户开放,请您登录
您对该条目有什么异议,请填写以下表单,管理员会尽快联系您。
内 容:
Email:  *
单位:
验证码:   刷新
您在IR的使用过程中有什么好的想法或者建议可以反馈给我们。
标 题:
 *
内 容:
Email:  *
验证码:   刷新

Items in IR are protected by copyright, with all rights reserved, unless otherwise indicated.

 

 

Valid XHTML 1.0!
Powered by CSpace