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题名: Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry
作者: Pang, Tao;  Yuan, Zhongyi;  Dai, Yongsheng;  Wang, Chang;  Yang, Jun;  Peng, Liming;  Xu, Guowang
通讯作者: 许国旺
关键词: APCI ;  glycosides ;  MS ;  tobacco
刊名: JOURNAL OF SEPARATION SCIENCE
发表日期: 2007-02-01
DOI: 10.1002/jssc.200600236
卷: 30, 期:3, 页:289-296
收录类别: SCI
文章类型: Article
部门归属: 18
项目归属: 1808
产权排名: 1;1
WOS标题词: Science & Technology ;  Physical Sciences
类目[WOS]: Chemistry, Analytical
研究领域[WOS]: Chemistry
英文摘要: HPLC-atmospheric pressure chemical ionization MS (HPLC-APCI-MS) was used to screen and identify glycosides in tobacco leaf. MS/MS and MS3 and photodiode array (PDA) detection were also used in the characterization. A total of 12 glycosides were found and four of them were identified based on their abundant [M + H](+) ions, UV and MS/MS analysis and they are scopolin, rutin, quercetin-3-glycoside, and spectra, kaempferol-3-rutino side. Analytical characteristics of the method were investigated. The contents of these glycosides were obtained and compared based on the relative peak area to the internal standard in seven kinds of tobacco leaf.
关键词[WOS]: FLAVONOID GLYCOSIDES ;  XANTHONE GLYCOSIDES ;  URINE SAMPLES ;  AGLYCONES ;  QUANTIFICATION ;  MS
语种: 英语
原文出处: 查看原文
WOS记录号: WOS:000244768400001
Citation statistics: 
内容类型: 期刊论文
URI标识: http://cas-ir.dicp.ac.cn/handle/321008/98795
Appears in Collections:中国科学院大连化学物理研究所_期刊论文

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作者单位: 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&D Ctr, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Biol Sci, Inst Biochem & Cell Biol, Shanghai, Peoples R China
3.Chuxiong Cigarette Co, Hongta Grp, Chuxiong, Yunnan, Peoples R China

Recommended Citation:
Pang, Tao,Yuan, Zhongyi,Dai, Yongsheng,et al. Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry[J]. JOURNAL OF SEPARATION SCIENCE,2007,30(3):289-296.
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